Bi-Material Micro-Part of Stainless Steel and Zirconia by Two-Component Micro-Powder Injection Molding: Rheological Properties and Solvent Debinding Behavior

Al Basir, Abu Bakar Sulong*, Nashrah Hani Jamadon and Norhamidi Muhamad

Abstract: From the micro-powder injection molding (microPIM) process, a two-component micro-powder injection molding (2C-microPIM) process has evolved due to the growing demand for multi-functional micro-components in avant-garde applications. 2C-microPIM technology provides the opportunity to conjugate distinct materials within one part. Stainless steel (SS 17-4PH) and 3 mol.% yttria-stabilized zirconia (3YSZ) are characteristically recognized for their corrosion resistance and high hardness. In this work, the obtained critical powder volume concentration (CPVC) of SS 17-4PH and 3YSZ powders were 71.7 and 47.1 vol.%, respectively. Solid loadings of 2 and 3 vol.% less than the CPVC were considered as the optimal content for both powders. Feedstocks were obtained by mixing SS 17-4PH and 3YSZ powders with a binder system comprised of palm stearin (PS) and low-density
polyethylene (LDPE). The rheological behaviors of the prepared feedstocks were assessed to figure
out the feedstocks having the best rheological properties. The feedstocks of SS 17-4PH and 3YSZ
with powder loadings of 69 and 44 vol.% were eventually injected to produce bi-material micro-parts.
The optimal solvent debinding temperature of the green bi-material micro-part was then investigated,
and it was found that 73.3% soluble binder was removed when bi-material was immersed in acetone
at 70 C for 40 min.

Professor Ir. Dr. Abu Bakar Sulong,
Department of Mechanical & Manufacturing Engineering,
Faculty of Engineering & Built Environment,
Universiti Kebangsaan Malaysia, 43600 Bangi, Selangor Darul Ehsan
Tel: +603-8921 6678
Fax: +603-8925 9659
Email: abubakar@ukm.edu.my, sulongabubakar@gmail.com

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