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UKM research instrumentation

Simultaneous Thermal Analyzer (STA)

BrandNETZSCH
ModelSTA 449 F3 Jupiter
LocationLevel 2, i-CRIM Centralised Lab, Centre for Natural and Physical Laboratory Management UKM (ALAF-UKM), Research Complex UKM
StatusAvailable

Overview

Simultaneous Thermal Analysis (STA) generally refers to the simultaneous application of Thermogravimetry (TGA) and Differential Scanning Calorimetry (DSC) to one and the same sample in a single instrument. The advantages are obvious: The test conditions are perfectly identical for the TGA and DSC signals (same atmosphere, gas flow rate, vapor pressure on the sample, heating rate, thermal contact to the sample crucible and sensor, radiation effect, etc.). Furthermore, sample throughput is improved as more information can be gathered from each test run.

Thermogravimetric analysis or thermal gravimetric analysis (TGA) is a method of thermal analysis in which the mass of a sample is measured over time as the temperature changes. This measurement provides information about physical phenomena, such as phase transitions, absorption, adsorption and desorption; as well as chemical phenomena including chemisorption, thermal decomposition, and solid-gas reactions (e.g., oxidation or reduction). A complementary DSC heat flow sensor simultaneously detects thermal events such as melting and crystallization in addition to providing accurate and precise transition temperatures.

Applications

Applications from the TGA include: compositional analysis, decomposition temperatures, engine oil volatility, flammability studies, lifetime predictions, measurement of volatiles, oxidative and thermal stabilities, and catalyst studies. 

Application from the DTA/DSC include: melting and crystallization behavior, glass transition temperatures, specific heat capacity, kinetic studies and transition and reaction enthalpies.

Sample Requirements

  • 1

    Powder

  • 2

    Solid

  • 3

    Liquid

Typical Results

Price List

Analysis Code Type of Analysis UKM Non-UKM
STA 01 Less than 800C RM120/analysis RM200/analysis
STA 02 More than 800C (max 1500C) RM150/analysis RM300/analysis
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Element List for ICPMS Analysis

  • Environmental Standard Elements

    Cr Mn Fe Cu Se Ni Zn As Ag Cd Sn Sb Ba Pb

  • Rare Earth Standard Elements

    Sc Y Ce La Nd Pr Eu Sm Tb Dy Er Yb Lu Gd Tm

  • Full Scan Elements

    Li Be B C N F Ne Na Mg Al Si P S Cl Ar K Ca Sc Ti V Cr Mn Fe Co Ni Cu Zn Ga Ge As Se Br Kr Rb Sr Y Zr Nb Mo Ru Rh Pd Ag Cd In Sn Sb Te I Xe Cs Ba La Ce Pr Nd Sm Eu Gd Tb Dy Ho Er Tm Yb Lu Hf Ta W Re Os Ir Pt Au Hg Tl Pb Bi Th U

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